Изучение взаимодействия в системе NaF-Bi2O3-BiF3 при 600 и 650 градусах Цельсия
Таблица 15. Результаты индицирования рентгенограммы фазы М в образце № 13(II).
Сингония – моноклинная.
Параметры ячейки:
a= 13.52(1) Å, b= 5.543(2) Å, c= 9.165(5) Å, b= 96.47(5)°
| N | 2*TH | D | I/I0 | Qobs | h | k | l | Qcalc | dQ |
| 1 | 17.248 | 5.13672 | 1 | 378.99 | 2 | 0 | 1 | 379.0 | -0.0 |
| 2 | 26.629 | 3.34463 | 5 | 893.93 | 1 | 1 | 2 | 899.9 | -6.0 |
| 3 | 29.377 | 3.03768 | 0 | 1083.72 | 0 | 0 | 3 | 1085.2 | -1.5 |
| 4 | 29.377 | 3.03768 | 0 | 1083.72 | -1 | 0 | 3 | 1085.3 | -1.6 |
| 5 | 29.544 | 3.02095 | 1 | 1095.75 | 3 | 0 | 2 | 1091.4 | 4.3 |
| 6 | 30.883 | 2.89294 | 3 | 1194.87 | 1 | 0 | 3 | 1195.8 | -0.9 |
| 7 | 30.883 | 2.89294 | 3 | 1194.87 | -2 | 0 | 3 | 1196.3 | -1.4 |
| 8 | 30.883 | 2.89294 | 3 | 1194.87 | -3 | 1 | 2 | 1195.9 | -1.0 |
| 9 | 42.266 | 2.13644 | 0 | 2190.88 | 4 | 0 | 3 | 2192.6 | -1.7 |
| 10 | 42.266 | 2.13644 | 0 | 2190.88 | 4 | 2 | 0 | 2188.1 | 2.8 |
| 11 | 43.338 | 2.08605 | 1 | 2298.01 | 2 | 0 | 4 | 2298.1 | -0.1 |
| 12 | 44.177 | 2.04834 | 2 | 2383.39 | 1 | 1 | 4 | 2383.7 | -0.3 |
| 13 | 50.392 | 1.80933 | 0 | 3054.67 | 3 | 2 | 3 | 3051.2 | 3.5 |
| 14 | 50.392 | 1.80933 | 0 | 3054.67 | -2 | 0 | 5 | 3051.9 | 2.8 |
| 15 | 50.392 | 1.80933 | 0 | 3054.67 | -4 | 2 | 3 | 3052.3 | 2.3 |
| 16 | 50.656 | 1.80050 | 0 | 3084.71 | -1 | 3 | 1 | 3086.3 | -1.6 |
| 17 | 52.418 | 1.74406 | 2 | 3287.59 | 7 | 1 | 1 | 3289.6 | -2.0 |
| 18 | 52.582 | 1.73900 | 0 | 3306.76 | 2 | 3 | 1 | 3307.7 | -1.0 |
| 19 | 64.392 | 1.44562 | 0 | 4785.08 | 2 | 0 | 6 | 4783.2 | 1.8 |
| 20 | 64.392 | 1.44562 | 0 | 4785.08 | -4 | 0 | 6 | 4785.3 | -0.2 |
| 21 | 64.392 | 1.44562 | 0 | 4785.08 | -6 | 1 | 5 | 4782.0 | 3.1 |
| 22 | 64.392 | 1.44562 | 0 | 4785.08 | -6 | 2 | 4 | 4783.5 | 1.6 |
| 23 | 69.754 | 1.34703 | 0 | 5511.23 | -2 | 4 | 1 | 5512.0 | -0.7 |
| 24 | 70.886 | 1.32827 | 0 | 5667.94 | 4 | 0 | 6 | 5669.0 | -1.1 |
| 25 | 70.886 | 1.32827 | 0 | 5667.94 | -6 | 0 | 6 | 5672.4 | -4.5 |
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